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گواهی نمایه سازی مقاله Efficient classical synthesis of aminoazines under microwave irradiation

عنوان مقاله: Efficient classical synthesis of aminoazines under microwave irradiation
شناسه (COI) مقاله: JR_ICC-2-2_008
منتشر شده در فصلنامه ارتباطات شیمی ایران در سال ۱۳۹۳
مشخصات نویسندگان مقاله:

Abbas Mohammadzadeh - Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran
Seyed Mohammad Vahdat - Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran
Esmaiel Derafshian - Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran
Somaieh Akhoondi - Department of Chemistry, Ayatollah Amoli Branch, Islamic Azad University, P.O. Box 678, Amol, Iran

خلاصه مقاله:
In the present study, Aminoazines were prepared from the reaction of amidrazone hydroiodide with various aromatic aldehydes in the presence of a solid base under microwave irradiation with power level of 850 W for 2-7 min in high yields. The amidrazone hydroiodide can also be prepared by the reaction of S-methyl isothiobenzamide hydroiodide and hydrazine in methanol under nitrogen gas. All synthesized compounds were characterized on the basis of IR and 1H NMR spectral data. The significant features of this method are short reaction times, high yields of the products, solvent free reaction, easy work-up procedure, direct production of aminoazines.

کلمات کلیدی:
Aminoazine, aldehyde, microwave irradiation.

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