Synthesis of Layered Double Hydroxide and Control of Crystal Structure by Hydrothermal Treatment under Reflux

In this study layered double hydroxide (LDH) nanoparticles were synthesized by a process involving co-precipitation using hydrothermal treatment under reflux(HTUR).Effect of HTUR conditioning on crystallinity of the LDH material was studied using Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction. We show that crystallinity of the obtained LDH increased with increase in HTUR time up to 24 hours

کلیدواژه ها:

Layered double hydroxide (LDH) ، Co-precipitation ، Crystallinity ، Hydrothermal Treatment ، Reflux