Synthesis of new lead(II) coordination polymer: New forerunner for production of pure phase lead(II) oxide nanoparticles via thermal decomposition
عنوان مقاله: Synthesis of new lead(II) coordination polymer: New forerunner for production of pure phase lead(II) oxide nanoparticles via thermal decomposition
شناسه ملی مقاله: ICNN05_244
منتشر شده در پنجمین کنگره بین المللی نانو و فناوری نانو (ICNN2014) در سال 1393
شناسه ملی مقاله: ICNN05_244
منتشر شده در پنجمین کنگره بین المللی نانو و فناوری نانو (ICNN2014) در سال 1393
مشخصات نویسندگان مقاله:
SeyedeRahele Nabavi - Department of chemistry, Tarbiat Modares University, Tehran, Iran
Ali Morsali - Department of chemistry, Tarbiat Modares University, Tehran, Iran
خلاصه مقاله:
SeyedeRahele Nabavi - Department of chemistry, Tarbiat Modares University, Tehran, Iran
Ali Morsali - Department of chemistry, Tarbiat Modares University, Tehran, Iran
New lead(II) nitrate coordination polymer [Pb(NO3)2(2-bpdb) (H2O)]n (1), (2-bpdb=1,4-bis(2-pyridyl)-3,4-diaza-1,3-butadiene) was synthesized.The compound 1 was characterized by IR spectroscopy.Pure phase PbO nano-particles were obtained by thermolyses of compound 1 in oleic acid as surfactant at180 and 200 ̊C under air atmosphere. The PbO nanoparticles were characterized by X-ray diffraction (XRD)and scanning electron microscopy (SEM).
کلمات کلیدی: Nano-particle, Lead(II), 1,4-bis(2-pyridyl)-3,4-diaza-1,3-butadiene, Crystal structure
صفحه اختصاصی مقاله و دریافت فایل کامل: https://civilica.com/doc/397433/